Aplikace transesterifikační derivatizační reakce pro GC-MS analýzy

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Publikace nespadá pod Fakultu sportovních studií, ale pod Přírodovědeckou fakultu. Oficiální stránka publikace je na webu muni.cz.
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BŘEZINA Adam DOŘMANOVÁ Adéla KUKUČKA Petr LUBAL Přemysl FARKOVÁ Marta

Rok publikování 2022
Druh Článek v odborném periodiku
Časopis / Zdroj Czech Chemical Society Symposium Series
Fakulta / Pracoviště MU

Přírodovědecká fakulta

Citace
www https://doi.org/10.54779/ccsss20220319
Doi http://dx.doi.org/10.54779/ccsss20220319
Popis This paper is focused on study of the concentration of the basic catalyst in methanol on the yield of the derivatization transesterification reaction of triacyglycerols. Potassium hydroxide and sodium hydroxide solutions were used as basic catalysts. Triacylglycerols were transesterified, rapeseed oil was used as a sample. Triacylglycerols were converted to methyl esters of fatty acids, which were subsequently determined by GC-MS where the peak areas were monitored, because they represent the yield of the formed fatty acid methyl esters, namely palmitic, oleic, linoleic and stearic acids. The highest yield of transesterification of the oil to methylesters of fatty acids was found for a concentration of 3.0 mol dm–3 for KOH and 2.0 mol dm–3 for NaOH. At higher catalyst concentrations, a predominant side-reaction, saponification, was observed, which decreased the overall yield of fatty acid methyl esters.
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