First Evidence of “Earth Wax” Inside the Casting Molds from the Roman Era
| Autoři | |
|---|---|
| Rok publikování | 2021 |
| Druh | Článek v odborném periodiku |
| Časopis / Zdroj | Molecules |
| Fakulta / Pracoviště MU | |
| Citace | |
| www | Full text |
| Doi | http://dx.doi.org/10.3390/molecules26144259 |
| Klíčová slova | earth wax; ceresin; soot; X-ray fluorescence; gas chromatography; Roman era; mold; mass spectrometry; ion mobility |
| Popis | This research was focused on the analysis of material composition and organic residues present in three molds found in the Moravian region (Czech Republic) belonging to the Roman era. X-ray fluorescence spectroscopy pointed out the possible remelting of Roman objects in Barbarian territory. The analysis of organic residues retrieved from the internal part of mold #2 by pyrolysisgas chromatography/mass spectrometry proved the presence of ozokerite wax (“earth wax”). Consequent analysis of this organic residue by Atmospheric Solids Analysis Probe–ion mobility spectrometry– high-resolution mass spectrometry (ASAP-IMS-HRMS) confirmed the presence of ceresin, the main component of ozokerite. Ceresin was also detected in a sample of the organic residue from mold #1. Note that this is the first application of ASAP-IMS-HRMS in archaeological research. The remains of earth wax in molds suggest the production of wax models as an intermediate stage for the production of lost-wax ceramic casting molds. |
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