HPLC separace chlorfenolů na koloně malého průměru pro stanovení v povrchových vodách
Title in English | HPLC Separation of Chlorophenols on Narrow-Bore Column for Their Determination in River Water |
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Authors | |
Year of publication | 2001 |
Type | Article in Proceedings |
Conference | Sborník 53. Zjazdu chemických spoločností |
MU Faculty or unit | |
Citation | |
Field | Analytic chemistry |
Keywords | Chlorophenols; HPLC; SPE; Narrow-Bore Column; River Water |
Description | Solid phase extraction of phenol and 15 chlorophenols from river water has been optimized and HPLC of the analytes on narrow-bore column has been investigated. The recoveries from 90% to 98% with exception of phenol (29%), pentachlorophenol (79%), and 2-chlorophenol (86%) were attained. Limits of detection ranged from 1.1 to 3.6 ug/L (5.2 for 2-chlorophenol and 14.6 for phenol) for the sample volume of 100 ml. |
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